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HPLC vs LC-MS for Peptide Analysis

HPLC and LC-MS answer different questions. HPLC reports how the main peak compares to other UV-detectable peaks. Liquid chromatography–mass spectrometry reports mass-to-charge information that supports identity of the main species.

Use HPLC when you need

  • A chromatogram and a relative purity figure for the tested lot
  • Lot-to-lot comparison under a stated method

Use LC-MS when you need

  • Evidence that the observed mass matches the expected peptide
  • Support for sequence-related identity claims beyond a single UV peak

A complete COA may include one or both. Revolution Peptide only repeats method names and values that appear on the attached certificate. We do not invent a second method if the PDF does not list it. Start with How to Read a Peptide COA and Understanding HPLC Peptide Purity.

Verification process: How Revolution Peptide Approaches Quality Verification. Documents: COA library.

Research use only. Analytical methods characterize laboratory materials. They are not treatment recommendations.

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